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Crystallization and preliminary X-ray diffraction analysis of FKBP12 complexed with a novel neurotrophic ligand. 2002
Pengyun Li, and
Liwei Wang, and
Yi Ding, and
Beili Wu, and
Cuiling Shu, and
Aihua Nie, and
Song Li, and
Beifen Shen, and
Zihe Rao
Laboratory of Structural Biology, Department of Biological Science and Technology & MOE Laboratory of Protein Science, Tsinghua University, Beijing 100084, China.
A novel neurotrophic ligand, (3R)-4-(p-Toluenesulfonyl)-1,4-thiazane-3-carboxylic acid-L-Leucine ethyl ester, has been complexed with FKBP12 and crystallized using the hanging-drop vapor-diffusion method. Crystals belong to P2(1) space group, with unit cell parameters a=41.2, b=29.6, c=41.5 A, beta=114.0 degrees. The crystals diffract to 1.8 A resolution limit.
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