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Calix[4]- and calix[5]arene-based multicavity macrocycles. 2002
Anna Notti, and
Salvatore Occhipinti, and
Sebastiano Pappalardo, and
Melchiorre F Parisi, and
Ilenia Pisagatti, and
Andrew J P White, and
David J Williams
Dipartimento di Chimica Organica e Biologica, Università di Messina, Salita Sperone 31, I-98166 Messina, Italy.
Synthesis and single-crystal X-ray structures of mixed triple and double calixarenes 6 and 7, obtained from the base-catalyzed condensation of calix[5]arene 1 with cone pertosylated calix[4]arene 2, are reported. VT-NMR studies on 7 are consistent with a molecular motion arising from the anti-gauche conformational interconversion of its ethylene linkages.
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