Spectroscopic studies on chromotropic mixed-ligand copper(II) complexes containing o-hydroxy benzoyl derivatives and dinitrogen bases. 2003

Ali Taha
Faculty of Education, Ain Shams University, Roxy, Cairo, Egypt. a.taha@uaeu.ac.ae <a.taha@uaeu.ac.ae>

Synthesis of chromotropic copper(II) mixed ligand complexes of o-hydroxy benzoyl derivatives (L1) and dinitrogen bases (L2), general formula Cun(L1)(L2)nXn; where n=1 or 2, L1=4,6-diacetyl-resorcinol (H2DACR), o-hydroxy benzaldhyde (HOHBZ) or o-hydroxy acetophenone (HOHAP), L2=N,N,N',N'-tetramethylethylenediamine (Me4en), 1,10-phenanthroline (phen) or bipyridine (bipy) and X=ClO4-, NO3- or Br- have been reported. Spectral, magnetic and molar conductance measurements as well as analytical data of these complexes show either mononuclear structure for OHBZ and OHAP or binuclear structure for DACR complexes. The IR stretching vibration frequencies of Cu-N and Cu-O are linearly correlated with the d-d absorption frequencies. The d-d absorption bands of Me4en-complexes in weak donor solvents suggest square-planar, distorted octahedral and distorted trigonal bipyramid geometries for the perchlorate, nitrate and bromide complexes, respectively. However, an octahedral structure is identified for the complexes in strong donor solvents. Perchlorate complexes show a remarkable color change from violet to green as the donor ability of the axial ligand increases, whereas bromide complexes are mainly affected by the Lewis acidity of the axial ligand. Specific and non-specific interactions of solvent molecules with the complexes are investigated using the unified solvation model. Calculations of the electronic transition probability (f) of the d-d band along with molecular orbital calculations of ligands have been carried out and correlated with the experimental data.

UI MeSH Term Description Entries
D008024 Ligands A molecule that binds to another molecule, used especially to refer to a small molecule that binds specifically to a larger molecule, e.g., an antigen binding to an antibody, a hormone or neurotransmitter binding to a receptor, or a substrate or allosteric effector binding to an enzyme. Ligands are also molecules that donate or accept a pair of electrons to form a coordinate covalent bond with the central metal atom of a coordination complex. (From Dorland, 27th ed) Ligand
D009942 Organometallic Compounds A class of compounds of the type R-M, where a C atom is joined directly to any other element except H, C, N, O, F, Cl, Br, I, or At. (Grant & Hackh's Chemical Dictionary, 5th ed) Metallo-Organic Compound,Metallo-Organic Compounds,Metalloorganic Compound,Organometallic Compound,Metalloorganic Compounds,Compound, Metallo-Organic,Compound, Metalloorganic,Compound, Organometallic,Compounds, Metallo-Organic,Compounds, Metalloorganic,Compounds, Organometallic,Metallo Organic Compound,Metallo Organic Compounds
D002863 Chromogenic Compounds Colorless, endogenous or exogenous pigment precursors that may be transformed by biological mechanisms into colored compounds; used in biochemical assays and in diagnosis as indicators, especially in the form of enzyme substrates. Synonym: chromogens (not to be confused with pigment-synthesizing bacteria also called chromogens). Chromogenic Compound,Chromogenic Substrate,Chromogenic Substrates,Compound, Chromogenic,Compounds, Chromogenic,Substrate, Chromogenic,Substrates, Chromogenic
D003300 Copper A heavy metal trace element with the atomic symbol Cu, atomic number 29, and atomic weight 63.55. Copper-63,Copper 63
D013816 Thermodynamics A rigorously mathematical analysis of energy relationships (heat, work, temperature, and equilibrium). It describes systems whose states are determined by thermal parameters, such as temperature, in addition to mechanical and electromagnetic parameters. (From Hawley's Condensed Chemical Dictionary, 12th ed) Thermodynamic
D015394 Molecular Structure The location of the atoms, groups or ions relative to one another in a molecule, as well as the number, type and location of covalent bonds. Structure, Molecular,Molecular Structures,Structures, Molecular
D017550 Spectroscopy, Fourier Transform Infrared A spectroscopic technique in which a range of wavelengths is presented simultaneously with an interferometer and the spectrum is mathematically derived from the pattern thus obtained. FTIR,Fourier Transform Infrared Spectroscopy,Spectroscopy, Infrared, Fourier Transform
D055672 Static Electricity The accumulation of an electric charge on a object Electrostatic,Electrostatics,Static Charge,Charge, Static,Charges, Static,Electricity, Static,Static Charges

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