Color stability and hardness in dental composites after accelerated aging. 2003

Karen A Schulze, and Sally J Marshall, and Stuart A Gansky, and Grayson W Marshall
Department of Preventive and Restorative Dental Sciences, Division of Biomaterials and Bioengineering, University of California San Francisco, 707 Parnassus Avenue, Box 0758, San Francisco, CA 94143-0758, USA.

OBJECTIVE To investigate the color and microhardness changes of five chemically- and five light-curing composites as a function of accelerated aging from light exposure. METHODS From each material five composite specimens were embedded in epoxy resin prior to determining the Knoop microhardness of the surface. For analyzing the color DeltaE*=f((L*a*b*)) with a spectrophotometer, three discs per composite were prepared. After measuring the baseline for hardness and color the same specimens were exposed to a xenon arc light and water in a Weather-Ometer machine for a total radiant energy of 150 kJ/m2 and 122 h. The microhardness and the color were again determined following the aging treatment. RESULTS Each material showed a significant increase in hardness after aging treatment (p<0.05). Comparing the hardness changes (in %) of the light-cured materials with the chemically cured materials, no significant difference could be found. Perceptible color differences could be observed for all the materials. Three brands showed small differences with DeltaE*=1.6-2.2, while four composites had DeltaE* ranging from 6.2 to 15.5. A significant correlation between hardness values and color changes could not be established. CONCLUSIONS The findings suggest that, since light-curable materials showed significantly more resistance to color changes after accelerated aging by light and water than chemically-cured materials, they may be more esthetically acceptable. Color changes were not correlated with surface hardness changes of the materials after aging.

UI MeSH Term Description Entries
D008027 Light That portion of the electromagnetic spectrum in the visible, ultraviolet, and infrared range. Light, Visible,Photoradiation,Radiation, Visible,Visible Radiation,Photoradiations,Radiations, Visible,Visible Light,Visible Radiations
D008422 Materials Testing The testing of materials and devices, especially those used for PROSTHESES AND IMPLANTS; SUTURES; TISSUE ADHESIVES; etc., for hardness, strength, durability, safety, efficacy, and biocompatibility. Biocompatibility Testing,Biocompatible Materials Testing,Hemocompatibility Testing,Testing, Biocompatible Materials,Testing, Hemocompatible Materials,Hemocompatibility Testings,Hemocompatible Materials Testing,Materials Testing, Biocompatible,Materials Testing, Hemocompatible,Testing, Biocompatibility,Testing, Hemocompatibility,Testing, Materials,Testings, Biocompatibility
D011108 Polymers Compounds formed by the joining of smaller, usually repeating, units linked by covalent bonds. These compounds often form large macromolecules (e.g., BIOPOLYMERS; PLASTICS). Polymer
D003116 Color The visually perceived property of objects created by absorption or reflection of specific wavelengths of light. Colors
D003188 Composite Resins Synthetic resins, containing an inert filler, that are widely used in dentistry. Composite Resin,Resin, Composite,Resins, Composite
D003799 Dental Stress Analysis The description and measurement of the various factors that produce physical stress upon dental restorations, prostheses, or appliances, materials associated with them, or the natural oral structures. Analyses, Dental Stress,Analysis, Dental Stress,Stress Analyses, Dental,Stress Analysis, Dental,Dental Stress Analyses
D006244 Hardness The mechanical property of material that determines its resistance to force. HARDNESS TESTS measure this property. Hardnesses
D006358 Hot Temperature Presence of warmth or heat or a temperature notably higher than an accustomed norm. Heat,Hot Temperatures,Temperature, Hot,Temperatures, Hot
D006813 Humidity A measure of the amount of WATER VAPOR in the air. Humidities
D000704 Analysis of Variance A statistical technique that isolates and assesses the contributions of categorical independent variables to variation in the mean of a continuous dependent variable. ANOVA,Analysis, Variance,Variance Analysis,Analyses, Variance,Variance Analyses

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