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Synthesis of new organic super acids-N-(trifluoromethylsulfonyl)imino derivatives of trifluoromethanesulfonic acid and bis(trifluoromethylsulfonyl)imide. 2005
Romute Yu Garlyauskayte, and
Alexander N Chernega, and
Christophe Michot, and
Michel Armand, and
Yurii L Yagupolskii, and
Lev M Yagupolskii
Institute of Organic Chemistry, National Academy of Sciences of Ukraine, 02094 Murmanskaya str. 5, Kiev, Ukraine. roma@bpci.kiev.ua
Salts of N-trifluoromethylsulfonyl derivatives of trifluoromethyl- and phenylsulfonimidoyl imides have been synthesized by two different routes. Both methods are one-pot reactions, that run in mild conditions with good yields. Two novel organic super acids: bis[N-(trifluoromethylsulfonyl)trifluoromethanesulfonimidoyl]imide and N,N'-bis(trifluoromethyl-sulfonyl)diimino trifluoromethanesulfonic acid were prepared and the structure of their potassium salts was obtained by single-crystal X-ray diffraction.
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