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Unexpected and expeditious entry into trifluoromethyl aziridines from substituted beta-dicarbonyl compounds. 2005
Dipartimento di Chimica, Università degli Studi La Sapienza, Piazzale Aldo Moro 2, I-00185 Roma, Italy.
[Reaction: see text]. One-pot aziridinations were obtained starting from substituted 2,2,2-trifluoroethyl beta-dicarbonyl compounds with nosyloxycarbamates in the presence of an excess of CaO as base. The unexpected ring closure reaction takes place at room temperature, leading to the N-protected alpha-trifluoromethyl aziridines with good yields. The reaction pathway seems to be influenced by the choice of the base.
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