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"O-acyl isopeptide method" for peptide synthesis: synthesis of forty kinds of "O-acyl isodipeptide unit" Boc-Ser/Thr(Fmoc-Xaa)-OH. 2007
Taku Yoshiya, and
Atsuhiko Taniguchi, and
Youhei Sohma, and
Fukue Fukao, and
Setsuko Nakamura, and
Naoko Abe, and
Nui Ito, and
Mariusz Skwarczynski, and
Tooru Kimura, and
Yoshio Hayashi, and
Yoshiaki Kiso
Department of Medicinal Chemistry, Center for frontier Research in Medicinal Science, 21st Century COE program, Kyoto Pharmaceutical University, Yamashina-ku, Kyoto 607-8412, Japan.
The O-acyl isopeptide method has recently received attention as an efficient synthetic method for peptides. Herein, forty kinds of "O-acyl isodipeptide unit" Boc-Ser/Thr(Fmoc-Xaa)-OH (1-40) were effectively synthesized in two-steps without epimerization. The O-acyl isodipeptide units are important building blocks to enable the routine use of the O-acyl isopeptide method.
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