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Screening for coumatetralyl in soft drinks by solid-matrix extraction and high-performance liquid chromatography with diode-array detection. 1991
A Dimuccio, and
I Camoni, and
L Vergori, and
R Dommarco, and
D Attard Barbini, and
F Vergori, and
A Ausili, and
A Santilio
Istituto Superiore di Sanità , Rome, Italy.
A method was developed for the rapid determination coumatetralyl in cola- and orange-type soft drinks, which includes extraction using solid-matrix column, clean-up by silica cartridge chromatography and reversed-phase high-performance liquid chromatography with diode-array detection. The recovery of coumatetralyl from 50 ml of soft drinks was better than 80% at spiking levels down to 50 micrograms/kg (ppb).
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