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Mesoporous NiO-Samaria doped ceria fuel cell materials. 2009

Tae Wook Eom, and Kyung Hwan Kim, and Jong Sung Kim, and Myung-Chan Jo, and Hyon Hee Yoon, and Sang Joon Park
Department of Chemical and Bio Engineering, Kyungwon University, Seongnam, 461-701, Korea.

The mesoporous NiO-SDC was synthesized using a cationic surfactant (cetyl-trimethylammonium bromide; CTAB) for obtaining wide triple-phase boundary (TPB) in solid oxide fuel cells (SOFCs). The microstructure of mesoporous NiO-SDC was characterized by XRD, SEM, BET, and HRTEM and the results showed that the mesoporous NiO-SDC with 6.3 nm pores could be obtained. After calcined at 600 degrees C, the surface area of NiO-SDC was 206 m2/g, which was sufficiently high for providing large TPB in SOFC anode. In addition, FT-IR measurements revealed that Ni(OH)2 and SDC were incorporated with amine group of CTAB.

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