The repair potential of resin composite materials. 2011

Chaiwat Maneenut, and Rangsima Sakoolnamarka, and Martin J Tyas
Faculty of Dentistry, Chulalongkorn University, Henri Dunant Rd, Bangkok, Thailand.

OBJECTIVE To measure the 'repair' strength of various combinations of composite using four manufacturers' adhesive systems, to compare the bond strengths with the cohesive strength of the original, unrepaired products and to assess whether the chemical nature of the resin matrix influenced the repair strength. METHODS Specimens were prepared of three composite materials Durafill, Heraeus Kulzer; P90 (Silorane) 3M ESPE; Z250 (3M ESPE) and aged in water at 60°C for 1 month. One surface of each specimen was faced with 80-grit silicone carbide paper, one of four adhesives placed (Ecusit, DMG; Clearfil Repair, Kuraray; P90 System Adhesive; Single Bond 2, 3M ESPE) and 'repair' composite added of the same type as above, such that all combinations of original and repair composite and adhesive were used. 'Stick' samples, approximately 6 mm × 0.8 mm × 4 mm were prepared from each repair specimen, a neck created at the junction of original and repair composites and the hour-glass sample tested in tension at 1 mm/min. The microtensile bond strength of the repair was calculated and the mode of failure (adhesive; cohesive in the original composite; cohesive in the repair composite) recorded. RESULTS There was no significant difference between the cohesive strengths of Filtek P90 and Filtek Z250 (both ≈106 MPa); both were significantly stronger than Durafill (67.0 MPa). For bonding to Durafill the bond strengths ranged from 17.6 MPa to 50.9 MPa; for bonding to P90, the bond strengths ranged from 5.0 MPa to 54.2 MPa; for bonding to Z250, the bond strengths ranged from 17.2 MPa to 75.4 MPa. Clearfil Repair appeared to provide the most consistently high bond strengths, followed by the P90 System Adhesive, Single Bond 2 and Ecusit. Overall, the majority of failures (74%) was adhesive. CONCLUSIONS It appears that bonding of new dimethacrylate-based composite to old dimethacrylate-based composite can be a viable clinical procedure. However, if the original composite is silorane-based (e.g., P90), then using the silane-based adhesive may be the best repair option, and similarly if it is planned to effect a repair with a silorane-based composite, using a silane-based adhesive may give the best outcome. The null hypotheses are thus rejected.

UI MeSH Term Description Entries
D008422 Materials Testing The testing of materials and devices, especially those used for PROSTHESES AND IMPLANTS; SUTURES; TISSUE ADHESIVES; etc., for hardness, strength, durability, safety, efficacy, and biocompatibility. Biocompatibility Testing,Biocompatible Materials Testing,Hemocompatibility Testing,Testing, Biocompatible Materials,Testing, Hemocompatible Materials,Hemocompatibility Testings,Hemocompatible Materials Testing,Materials Testing, Biocompatible,Materials Testing, Hemocompatible,Testing, Biocompatibility,Testing, Hemocompatibility,Testing, Materials,Testings, Biocompatibility
D008689 Methacrylates Acrylic acids or acrylates which are substituted in the C-2 position with a methyl group. Methacrylate
D001840 Dental Bonding An adhesion procedure for orthodontic attachments, such as plastic DENTAL CROWNS. This process usually includes the application of an adhesive material (DENTAL CEMENTS) and letting it harden in-place by light or chemical curing. Bonding, Dental,Cure of Orthodontic Adhesives,Curing, Dental Cement,Dental Cement Curing,Orthodontic Adhesives Cure
D003188 Composite Resins Synthetic resins, containing an inert filler, that are widely used in dentistry. Composite Resin,Resin, Composite,Resins, Composite
D003738 Dental Cements Substances used to bond COMPOSITE RESINS to DENTAL ENAMEL and DENTIN. These bonding or luting agents are used in restorative dentistry, ROOT CANAL THERAPY; PROSTHODONTICS; and ORTHODONTICS. Dental Adhesives,Luting Agents,Orthodontic Adhesives,Cement, Dental,Cements, Dental,Dental Cement,Adhesive, Dental,Adhesive, Orthodontic,Adhesives, Dental,Adhesives, Orthodontic,Dental Adhesive,Luting Agent,Orthodontic Adhesive
D003764 Dental Materials Materials used in the production of dental bases, restorations, impressions, prostheses, etc. Dental Material,Material, Dental,Materials, Dental
D003799 Dental Stress Analysis The description and measurement of the various factors that produce physical stress upon dental restorations, prostheses, or appliances, materials associated with them, or the natural oral structures. Analyses, Dental Stress,Analysis, Dental Stress,Stress Analyses, Dental,Stress Analysis, Dental,Dental Stress Analyses
D006801 Humans Members of the species Homo sapiens. Homo sapiens,Man (Taxonomy),Human,Man, Modern,Modern Man
D000134 Acid Etching, Dental Preparation of TOOTH surfaces and DENTAL MATERIALS with etching agents, usually phosphoric acid, to roughen the surface to increase adhesion or osteointegration. Dental Acid Etching,Etching, Dental Acid
D000268 Adhesiveness A property of the surface of an object that makes it stick to another surface. Adhesivenesses

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