[Adsorption performances for sulfur dioxide using imidazole ionic liquids]. 2010

Yao-Xu Tang, and Wei-Kun Mao, and Na Ma, and Xiao-Fan Zhu, and Jian Hua, and Hua-Qiang Yin
College of Light Industry, Textile and Food Engineering, Sichuan University, Chengdu 610065, China. tyaoxu@tom.com

To discover the SO2 adsorption laws of ionic liquids in simulating flue gas, the SO2 adsorbents 1-butyl-3-methylimidazolium chloride ([Bmim] Cl), 1-butyl-3-methylimidazolium nitrate ([Bmim] NO3), 1-butyl-3-methylimidazolium tetrafluoroborate ([Bmim] BF4) and 1-amyl-3-methylimidazolium chloride [C5 mim] Cl ionic liquids were synthesized. The performances were studied under different conditions and the general rules of regeneration were explored. And the diversification of [Bmim] Cl chemical structures, which were pre-desulfated, post-desulfated and post-regenerated, were characterized by Fourier Transform Infrared Spectroscopy. The results illustrated that these ionic liquids all had the ability of SO2 adsorption, and the order of SO2 adsorption performances was [C5 mim] C1 > [Bmim] Cl > [Bmim] NO3 > [Bmim] BF4. The total SO2 adsorption amount of [C5 mim] Cl was 200. 8 mg/g, and the optimal adsorption temperature of [Bmim] Cl was 40 degrees C. The order of anions impacting adsorption performances of ionic liquids was Cl- > NO3- > BF4-. The sulfur capacity of ionic liquids decreased to 26.5 mg/g from 65.9 mg/g after desorption under the condition of heating (90 degrees C), vacuum (0.09 MPa) and 4.0 h. In addition, the chemical structures of ionic liquid had changed, and the forms of SO2 adsorbed by [Bmim] Cl were physico-chemical processes.

UI MeSH Term Description Entries
D007093 Imidazoles Compounds containing 1,3-diazole, a five membered aromatic ring containing two nitrogen atoms separated by one of the carbons. Chemically reduced ones include IMIDAZOLINES and IMIDAZOLIDINES. Distinguish from 1,2-diazole (PYRAZOLES).
D000327 Adsorption The adhesion of gases, liquids, or dissolved solids onto a surface. It includes adsorptive phenomena of bacteria and viruses onto surfaces as well. ABSORPTION into the substance may follow but not necessarily. Adsorptions
D000393 Air Pollutants Any substance in the air which could, if present in high enough concentration, harm humans, animals, vegetation or materials. Substances include GASES; PARTICULATE MATTER; and volatile ORGANIC CHEMICALS. Air Pollutant,Air Pollutants, Environmental,Environmental Air Pollutants,Environmental Pollutants, Air,Air Environmental Pollutants,Pollutant, Air,Pollutants, Air,Pollutants, Air Environmental,Pollutants, Environmental Air
D013458 Sulfur Dioxide A highly toxic, colorless, nonflammable gas. It is used as a pharmaceutical aid and antioxidant. It is also an environmental air pollutant. Sulfurous Anhydride
D052578 Ionic Liquids Salts that melt below 100 C. Their low VOLATILIZATION can be an advantage over volatile organic solvents. Ionic Liquid,Ionic Solvents,Liquid, Ionic,Liquids, Ionic,Solvents, Ionic

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