BIOMAT Database Logo BIOMAT Database Logo

1-[5-Acetyl-4-(4-bromo-phen-yl)-2,6-dimethyl-1,4-dihydro-pyridin-3-yl]ethanone monohydrate. 2010

Palakshi B Reddy, and V Vijayakumar, and S Sarveswari, and T Narasimhamurthy, and Edward R T Tiekink

The 1,4-dihydro-pyridine ring in the title hydrate, C(17)H(18)BrNO(2)·H(2)O, has a flattened-boat conformation, and the benzene ring is occupies a position orthogonal to this [dihedral angle: 82.19 (16)°]. In the crystal packing, supra-molecular arrays mediated by N-H⋯O(water) and O(water)-H⋯O(carbon-yl) hydrogen bonding are formed in the bc plane. A highly disordered solvent mol-ecule is present within a mol-ecular cavity defined by the organic and water mol-ecules. Its contribution to the electron density was removed from the observed data in the final cycles of refinement and the formula, mol-ecular weight and density are given without taking into account the contribution of the solvent mol-ecule.

UI MeSH Term Description Entries

Related Publications

Palakshi B Reddy, and V Vijayakumar, and S Sarveswari, and T Narasimhamurthy, and Edward R T Tiekink
1-[5-Acetyl-2,6-dimethyl-4-(5-phenyl-1H-pyrazol-3-yl)-1,4-dihydro-pyridin-3-yl]ethanone monohydrate.
November 2012, Acta crystallographica. Section E, Structure reports online,
Palakshi B Reddy, and V Vijayakumar, and S Sarveswari, and T Narasimhamurthy, and Edward R T Tiekink
1-[5-(4-Bromo-phen-yl)-3-(4-fluoro-phen-yl)-4,5-dihydro-1H-pyrazol-1-yl]ethanone.
August 2012, Acta crystallographica. Section E, Structure reports online,
Palakshi B Reddy, and V Vijayakumar, and S Sarveswari, and T Narasimhamurthy, and Edward R T Tiekink
Dimethyl 2,6-dimethyl-4-{3-[4-(methyl-sulfan-yl)phen-yl]-1H-pyrazol-4-yl}-1,4-dihydro-pyridine-3,5-dicarboxyl-ate monohydrate.
December 2012, Acta crystallographica. Section E, Structure reports online,
Palakshi B Reddy, and V Vijayakumar, and S Sarveswari, and T Narasimhamurthy, and Edward R T Tiekink
3,5-Bis[1-acetyl-5-(4-chloro-phen-yl)-4,5-dihydro-1H-pyrazol-3-yl]-2,6-dimethyl-pyridine.
August 2008, Acta crystallographica. Section E, Structure reports online,
Palakshi B Reddy, and V Vijayakumar, and S Sarveswari, and T Narasimhamurthy, and Edward R T Tiekink
3-(4-Bromo-phen-yl)-5-[4-(dimethyl-amino)-phen-yl]-4,5-dihydro-1H-pyrazole-1-carbothio-amide.
February 2011, Acta crystallographica. Section E, Structure reports online,
Palakshi B Reddy, and V Vijayakumar, and S Sarveswari, and T Narasimhamurthy, and Edward R T Tiekink
Dimethyl 4-(3-hydroxy-phen-yl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxyl-ate.
March 2010, Acta crystallographica. Section E, Structure reports online,
Palakshi B Reddy, and V Vijayakumar, and S Sarveswari, and T Narasimhamurthy, and Edward R T Tiekink
Diisopropyl 1-(4-meth-oxy-phen-yl)-2,6-dimethyl-4-(3-nitro-phen-yl)-1,4-dihydro-pyridine-3,5-dicarboxyl-ate.
November 2011, Acta crystallographica. Section E, Structure reports online,
Palakshi B Reddy, and V Vijayakumar, and S Sarveswari, and T Narasimhamurthy, and Edward R T Tiekink
1-Bromo-acetyl-2,6-bis-(4-methoxy-phen-yl)-3,5-dimethyl-piperidin-4-one.
September 2008, Acta crystallographica. Section E, Structure reports online,
Palakshi B Reddy, and V Vijayakumar, and S Sarveswari, and T Narasimhamurthy, and Edward R T Tiekink
1-[5-(4-Chloro-phen-yl)-3-(4-hy-droxy-phen-yl)-4,5-dihydro-1H-pyrazol-1-yl]-ethanone.
March 2012, Acta crystallographica. Section E, Structure reports online,
Palakshi B Reddy, and V Vijayakumar, and S Sarveswari, and T Narasimhamurthy, and Edward R T Tiekink
1-[3-(4-Chloro-phen-yl)-5-(4-meth-oxy-phen-yl)-4,5-dihydro-1H-pyrazol-1-yl]ethanone.
April 2012, Acta crystallographica. Section E, Structure reports online,
Copied contents to your clipboard!