BIOMAT Database Logo BIOMAT Database Logo

tert-Butyl 2-{[2,8-bis-(trifluoro-meth-yl)quinolin-4-yl](hy-droxy)meth-yl}piperidine-1-carboxyl-ate. 2011

Raoni S B Gonçalves, and Marcus V N de Souza, and James L Wardell, and Solange M S V Wardell, and Edward R T Tiekink

The title mol-ecule, C(22)H(24)F(6)N(2)O(3), adopts a folded conformation whereby the carboxyl-ate residue lies over the quinolinyl residue, with the dihedral angle between the carbamate and quinoline planes being 41.64 (7)°. Helical supra-molecular C(7) chains sustained by O-H⋯O hydrogen bonds propagating along the a-axis direction feature in the crystal packing. The F atoms of one of the CF(3) groups are disordered over two orientations; the major component has a site occupancy of 0.824 (7).

UI MeSH Term Description Entries

Related Publications

Raoni S B Gonçalves, and Marcus V N de Souza, and James L Wardell, and Solange M S V Wardell, and Edward R T Tiekink
tert-Butyl 1-hy-droxy-piperidine-2-carboxyl-ate.
August 2011, Acta crystallographica. Section E, Structure reports online,
Raoni S B Gonçalves, and Marcus V N de Souza, and James L Wardell, and Solange M S V Wardell, and Edward R T Tiekink
2-{[2,8-Bis(trifluoro-meth-yl)quinolin-4-yl](hy-droxy)meth-yl}piperidin-1-ium 3-amino-5-nitro-benzoate sesquihydrate.
November 2011, Acta crystallographica. Section E, Structure reports online,
Raoni S B Gonçalves, and Marcus V N de Souza, and James L Wardell, and Solange M S V Wardell, and Edward R T Tiekink
tert-Butyl 4-{[2-amino-4-(2-hy-droxy-phen-yl)pyrimidin-5-yl]meth-yl}piperazine-1-carboxyl-ate.
January 2013, Acta crystallographica. Section E, Structure reports online,
Raoni S B Gonçalves, and Marcus V N de Souza, and James L Wardell, and Solange M S V Wardell, and Edward R T Tiekink
Methyl 2-{[2,8-bis-(trifluoro-meth-yl)quinolin-4-yl]-oxy}acetate.
January 2011, Acta crystallographica. Section E, Structure reports online,
Raoni S B Gonçalves, and Marcus V N de Souza, and James L Wardell, and Solange M S V Wardell, and Edward R T Tiekink
Nicotinaldehyde [2,8-bis-(trifluoro-meth-yl)quinolin-4-yl]hydrazone monohydrate.
August 2010, Acta crystallographica. Section E, Structure reports online,
Raoni S B Gonçalves, and Marcus V N de Souza, and James L Wardell, and Solange M S V Wardell, and Edward R T Tiekink
(E)-tert-Butyl 4-(N'-hy-droxy-carbam--imid-o-yl)piperazine-1-carboxyl-ate.
December 2012, Acta crystallographica. Section E, Structure reports online,
Raoni S B Gonçalves, and Marcus V N de Souza, and James L Wardell, and Solange M S V Wardell, and Edward R T Tiekink
Crystal structure and Hirshfeld surface analysis of 2-{[2,8-bis-(tri-fluoro-meth-yl)quinolin-4-yl](hy-droxy)meth-yl}piperidin-1-ium 2-hy-droxy-2-phenyl-acetate hemihydrate.
November 2016, Acta crystallographica. Section E, Crystallographic communications,
Raoni S B Gonçalves, and Marcus V N de Souza, and James L Wardell, and Solange M S V Wardell, and Edward R T Tiekink
Bis(2-{[2,8-bis-(trifluoro-meth-yl)quinolin-4-yl](hydr-oxy)meth-yl}piperidin-1-ium) tetra-chloridodiphenyl-stannate(IV).
February 2010, Acta crystallographica. Section E, Structure reports online,
Raoni S B Gonçalves, and Marcus V N de Souza, and James L Wardell, and Solange M S V Wardell, and Edward R T Tiekink
[6-(Hy-droxy-meth-yl)pyridin-2-yl]methyl ferrocene-1-carboxyl-ate.
November 2011, Acta crystallographica. Section E, Structure reports online,
Raoni S B Gonçalves, and Marcus V N de Souza, and James L Wardell, and Solange M S V Wardell, and Edward R T Tiekink
Ethyl 6-(4-fluoro-phen-yl)-4-hy-droxy-2-oxo-4-trifluoro-meth-yl-1,3-diazinane-5-carboxyl-ate monohydrate.
July 2011, Acta crystallographica. Section E, Structure reports online,
Copied contents to your clipboard!