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Dynamic nuclear polarization of quadrupolar nuclei using cross polarization from protons: surface-enhanced aluminium-27 NMR. 2012
Veronika Vitzthum, and
Pascal Miéville, and
Diego Carnevale, and
Marc A Caporini, and
David Gajan, and
Christophe Copéret, and
Moreno Lelli, and
Alexandre Zagdoun, and
Aaron J Rossini, and
Anne Lesage, and
Lyndon Emsley, and
Geoffrey Bodenhausen
Institut des Sciences et Ingénierie Chimiques, Ecole Polytechnique Fédérale de Lausanne, EPFL, Batochime, 1015 Lausanne, Switzerland.
The surface of γ-alumina nanoparticles can be characterized by dynamic nuclear polarization (DNP) surface-enhanced NMR of (27)Al. DNP is combined with cross-polarization and MQ-MAS to determine local symmetries of (27)Al sites at the surface.
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