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Pd-catalyzed domino carbonylative-decarboxylative allylation: an easy and selective monoallylation of ketones. 2012
Steven Giboulot, and
Frédéric Liron, and
Guillaume Prestat, and
Benoit Wahl, and
Mathieu Sauthier, and
Yves Castanet, and
André Mortreux, and
Giovanni Poli
UPMC, IPCM, UMR CNRS 7201, 4 place Jussieu, case 183, F-75252 Paris Cedex 05, France.
In the presence of an allyl alcohol, α-chloroacetophenones undergo an allyloxycarbonylation reaction followed by in situ decarboxylative allylation to selectively afford the corresponding monoallylated ketones via a Pd-catalyzed domino sequence. The scope of the reaction was extended to substituted α-chloroacetophenones as well as various allyl alcohols.
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