In this article we report that peroxidlipid in edible oil-fats is extracted by using thylene glycol and measured by using TBA colorimetric method. This method is simple, rapid and has a high degree of accuracy with CV of 4.5%. The contents of peroxidlipid have been studied for certain edible oil-fats before and after high heat. The results showed that the contents of LPO were markedly increased after high heating.