Photocatalytic reduction of Cr(VI) by small molecular weight organic acids over schwertmannite. 2012

Danjun Jiang, and Ying Li, and Yong Wu, and Pei Zhou, and Yeqing Lan, and Lixiang Zhou
College of Sciences, Nanjing Agricultural University, Nanjing, PR China.

In this study, a series of bath experiments was carried out to investigate the photoreduction of Cr(VI) by small molecular weight organic acids (SOAs) over schwertmannite, a mineral found in acid mine drainage (AMD). The results demonstrated that schwertmannite or SOAs alone was unable to effectively transform Cr(VI) to Cr(III) even if exposed to an illumination of mimic solar light. However, an addition of schwertmannite significantly enhanced the reduction of Cr(VI) by SOAs under the same condition. For example, 100μM Cr(VI) was almost completely removed within 50min in the presence of both schwertmannite (0.6gL(-1)) and oxalic acid (300μM) at pH 3.0. The photocatalytic reduction of Cr(VI) was strongly influenced by pH, the initial concentrations and the structures of SOAs. Of the tested three SOAs, the reaction rates of photocatalytic reduction of Cr(VI) were in the order of oxalic acid>citric acid>tartaric acid. The reaction obeyed to zero-order kinetics with respect to Cr(VI) with excess SOAs. A possible mechanism for photoreduction of Cr(VI) by SOAs over schwertmannite was proposed. Fe(III) on the surface of schwertmannite was dissolved by SOAs, and then Fe(III)-SOA complexes with high photochemical activity formed. Further, Fe(II) together with organic acid radicals, CO(2)(-) and O(2)(-), was generated through a metal-ligand-charge-transfer pathway (MLCT), leading to a rapid reduction of Cr(VI).

UI MeSH Term Description Entries
D007700 Kinetics The rate dynamics in chemical or physical systems.
D008027 Light That portion of the electromagnetic spectrum in the visible, ultraviolet, and infrared range. Light, Visible,Photoradiation,Radiation, Visible,Visible Radiation,Photoradiations,Radiations, Visible,Visible Light,Visible Radiations
D010084 Oxidation-Reduction A chemical reaction in which an electron is transferred from one molecule to another. The electron-donating molecule is the reducing agent or reductant; the electron-accepting molecule is the oxidizing agent or oxidant. Reducing and oxidizing agents function as conjugate reductant-oxidant pairs or redox pairs (Lehninger, Principles of Biochemistry, 1982, p471). Redox,Oxidation Reduction
D002384 Catalysis The facilitation of a chemical reaction by material (catalyst) that is not consumed by the reaction. Catalyses
D002857 Chromium A trace element that plays a role in glucose metabolism. It has the atomic symbol Cr, atomic number 24, and atomic weight 52. According to the Fourth Annual Report on Carcinogens (NTP85-002,1985), chromium and some of its compounds have been listed as known carcinogens.
D005290 Ferric Compounds Inorganic or organic compounds containing trivalent iron. Compounds, Ferric
D006863 Hydrogen-Ion Concentration The normality of a solution with respect to HYDROGEN ions; H+. It is related to acidity measurements in most cases by pH pH,Concentration, Hydrogen-Ion,Concentrations, Hydrogen-Ion,Hydrogen Ion Concentration,Hydrogen-Ion Concentrations
D013644 Tartrates Derivatives of tartronic acid (the structural formula (COOH)CHOH(COOH)) including its salts and esters.
D056831 Coordination Complexes Neutral or negatively charged ligands bonded to metal cations or neutral atoms. The number of ligand atoms to which the metal center is directly bonded is the metal cation's coordination number, and this number is always greater than the regular valence or oxidation number of the metal. A coordination complex can be negative, neutral, or positively charged. Metal Complexes,Complexes, Coordination,Complexes, Metal
D058085 Iron Compounds Organic and inorganic compounds that contain iron as an integral part of the molecule. Compounds, Iron

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