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Synthesis and characterization of isomerically pure anti- and syn-anthradiindole derivatives. 2013
Jean-Yves Balandier, and
Nicolas Henry, and
Jean-Baptiste Arlin, and
Lionel Sanguinet, and
Vincent Lemaur, and
Claude Niebel, and
Basab Chattopadhyay, and
Alan Robert Kennedy, and
Philippe Leriche, and
Philippe Blanchard, and
Jérôme Cornil, and
Yves Henri Geerts
Université Libre de Bruxelles (ULB), Faculté des Sciences, Laboratoire Chimie des Polymères, CP 206/1, Boulevard du Triomphe, 1050 Bruxelles, Belgium. jbalandi@ulb.ac.be
Synthesis, isolation, and characterization of isomerically pure syn- and anti-anthradiindole (ADI) derivatives are described. The anti- and syn-ADI structures are demonstrated by (13)C NMR spectroscopy and by single-crystal X-ray diffraction. The spectroscopic and electrochemical properties as well as the stability of these newly synthesized π-conjugated systems are evaluated and supported by quantum-chemical calculations.
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