BIOMAT Database Logo BIOMAT Database Logo

Evaluation of matrix solid-phase dispersion (MSPD) extraction for multi-fenicols determination in shrimp and fish by liquid chromatography-electrospray ionisation tandem mass spectrometry. 2014

Yanfei Tao, and Fangwei Zhu, and Dongmei Chen, and Huimin Wei, and Yuanhu Pan, and Xu Wang, and Zhenli Liu, and Lingli Huang, and Yulian Wang, and Zonghui Yuan
National Reference Laboratory of Veterinary Drug Residues (HZAU)/MOA Key Laboratory of Food Safety Evaluation, Huazhong Agricultural University, Wuhan 430070, China.

A quantitative LC-MS/MS method was developed for the determination of chloramphenicol (CAP), thiamphenicol (TAP), florfenicol (FF) and florfenicol amine (FFA) in shrimp and fish. This rapid simple and effective extraction method was based on matrix solid-phase dispersion (MSPD). The best results were obtained using C18 as dispersant sorbent. The correlation coefficient (r) with each matrix-matched calibration curve is higher than 0.999 at the range of 0.05-0.8μg/kg for CAP and FF, 0.1-1.6μg/kg for FFA and TAP. CCα and CCβ of the fenicols upon the method were ranged from 0.01 to 0.09μg/kg and 0.04 to 0.25μg/kg respectively. In the fortified levels recoveries of the four compounds ranged from 83.8% to 98.8% with RSDs lower than 13.7%. The proposed method has been applied successfully to the analysis of CAP, TAP, FF and FFA in shrimp and fish samples, which demonstrates that this method is fast, sensitive, reliable and environmental friendly.

UI MeSH Term Description Entries
D002701 Chloramphenicol An antibiotic first isolated from cultures of Streptomyces venequelae in 1947 but now produced synthetically. It has a relatively simple structure and was the first broad-spectrum antibiotic to be discovered. It acts by interfering with bacterial protein synthesis and is mainly bacteriostatic. (From Martindale, The Extra Pharmacopoeia, 29th ed, p106) Cloranfenicol,Kloramfenikol,Levomycetin,Amphenicol,Amphenicols,Chlornitromycin,Chlorocid,Chloromycetin,Detreomycin,Ophthochlor,Syntomycin
D002853 Chromatography, Liquid Chromatographic techniques in which the mobile phase is a liquid. Liquid Chromatography
D003445 Crustacea A large subphylum of mostly marine ARTHROPODS containing over 42,000 species. They include familiar arthropods such as lobsters (NEPHROPIDAE), crabs (BRACHYURA), shrimp (PENAEIDAE), and barnacles (THORACICA). Ostracoda,Ostracods,Crustaceas,Ostracod,Ostracodas
D005399 Fishes A group of cold-blooded, aquatic vertebrates having gills, fins, a cartilaginous or bony endoskeleton, and elongated bodies covered with scales.
D000818 Animals Unicellular or multicellular, heterotrophic organisms, that have sensation and the power of voluntary movement. Under the older five kingdom paradigm, Animalia was one of the kingdoms. Under the modern three domain model, Animalia represents one of the many groups in the domain EUKARYOTA. Animal,Metazoa,Animalia
D000900 Anti-Bacterial Agents Substances that inhibit the growth or reproduction of BACTERIA. Anti-Bacterial Agent,Anti-Bacterial Compound,Anti-Mycobacterial Agent,Antibacterial Agent,Antibiotics,Antimycobacterial Agent,Bacteriocidal Agent,Bacteriocide,Anti-Bacterial Compounds,Anti-Mycobacterial Agents,Antibacterial Agents,Antibiotic,Antimycobacterial Agents,Bacteriocidal Agents,Bacteriocides,Agent, Anti-Bacterial,Agent, Anti-Mycobacterial,Agent, Antibacterial,Agent, Antimycobacterial,Agent, Bacteriocidal,Agents, Anti-Bacterial,Agents, Anti-Mycobacterial,Agents, Antibacterial,Agents, Antimycobacterial,Agents, Bacteriocidal,Anti Bacterial Agent,Anti Bacterial Agents,Anti Bacterial Compound,Anti Bacterial Compounds,Anti Mycobacterial Agent,Anti Mycobacterial Agents,Compound, Anti-Bacterial,Compounds, Anti-Bacterial
D012758 Shellfish Aquatic invertebrates belonging to the phylum MOLLUSCA or the subphylum CRUSTACEA, and used as food.
D013839 Thiamphenicol A methylsulfonyl analog of CHLORAMPHENICOL. It is an antibiotic and immunosuppressive agent. Dextrosulfenidol,Thiophenicol,Raceophenidol,Thiamcol,Thiomycetin,Urfamycin,Vicemycetin
D017747 Seafood Marine fish and shellfish used as food or suitable for food. (Webster, 3d ed) SHELLFISH and FISH PRODUCTS are more specific types of SEAFOOD. Sea-Food,Sea Food,Sea-Foods,Seafoods
D052616 Solid Phase Extraction An extraction method that separates analytes using a solid phase and a liquid phase. It is used for preparative sample cleanup before analysis by CHROMATOGRAPHY and other analytical methods. Extraction, Solid Phase,Extractions, Solid Phase,Solid Phase Extractions

Related Publications

Yanfei Tao, and Fangwei Zhu, and Dongmei Chen, and Huimin Wei, and Yuanhu Pan, and Xu Wang, and Zhenli Liu, and Lingli Huang, and Yulian Wang, and Zonghui Yuan
[Determination of the thyreostats in animal muscle tissue by matrix solid-phase dispersion (MSPD) and liquid chromatography-tandem mass spectrometry].
January 2012, Roczniki Panstwowego Zakladu Higieny,
Yanfei Tao, and Fangwei Zhu, and Dongmei Chen, and Huimin Wei, and Yuanhu Pan, and Xu Wang, and Zhenli Liu, and Lingli Huang, and Yulian Wang, and Zonghui Yuan
Determination of chemotherapeutic agents in fish and shellfish by matrix solid-phase dispersion and liquid chromatography-tandem mass spectrometry.
November 2012, Journal of separation science,
Yanfei Tao, and Fangwei Zhu, and Dongmei Chen, and Huimin Wei, and Yuanhu Pan, and Xu Wang, and Zhenli Liu, and Lingli Huang, and Yulian Wang, and Zonghui Yuan
[Determination of gibberellins in Arabidopsis thaliana by matrix solid-phase dispersion extraction and high performance liquid chromatography-tandem mass spectrometry].
September 2011, Se pu = Chinese journal of chromatography,
Yanfei Tao, and Fangwei Zhu, and Dongmei Chen, and Huimin Wei, and Yuanhu Pan, and Xu Wang, and Zhenli Liu, and Lingli Huang, and Yulian Wang, and Zonghui Yuan
Determination of several pesticides in water by solid-phase extraction, liquid chromatography and electrospray tandem mass spectrometry.
May 2007, Journal of chromatography. A,
Yanfei Tao, and Fangwei Zhu, and Dongmei Chen, and Huimin Wei, and Yuanhu Pan, and Xu Wang, and Zhenli Liu, and Lingli Huang, and Yulian Wang, and Zonghui Yuan
Determination of perfluorinated compounds in mollusks by matrix solid-phase dispersion and liquid chromatography-tandem mass spectrometry.
January 2012, Analytical and bioanalytical chemistry,
Yanfei Tao, and Fangwei Zhu, and Dongmei Chen, and Huimin Wei, and Yuanhu Pan, and Xu Wang, and Zhenli Liu, and Lingli Huang, and Yulian Wang, and Zonghui Yuan
Simultaneous determination of ten steroid hormones in animal origin food by matrix solid-phase dispersion and liquid chromatography-electrospray tandem mass spectrometry.
January 2014, Food chemistry,
Yanfei Tao, and Fangwei Zhu, and Dongmei Chen, and Huimin Wei, and Yuanhu Pan, and Xu Wang, and Zhenli Liu, and Lingli Huang, and Yulian Wang, and Zonghui Yuan
Determination of Bile Acids in Piglet Bile by Solid Phase Extraction and Liquid Chromatography-Electrospray Tandem Mass Spectrometry.
March 2016, Lipids,
Yanfei Tao, and Fangwei Zhu, and Dongmei Chen, and Huimin Wei, and Yuanhu Pan, and Xu Wang, and Zhenli Liu, and Lingli Huang, and Yulian Wang, and Zonghui Yuan
Determination of 4-Hexylresorcinol in Shrimp Samples by Solid Phase Extraction Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry.
August 2018, Molecules (Basel, Switzerland),
Yanfei Tao, and Fangwei Zhu, and Dongmei Chen, and Huimin Wei, and Yuanhu Pan, and Xu Wang, and Zhenli Liu, and Lingli Huang, and Yulian Wang, and Zonghui Yuan
Rapid assay for analyzing biogenic amines in cheese: matrix solid-phase dispersion followed by liquid chromatography-electrospray-tandem mass spectrometry.
May 2005, Journal of agricultural and food chemistry,
Yanfei Tao, and Fangwei Zhu, and Dongmei Chen, and Huimin Wei, and Yuanhu Pan, and Xu Wang, and Zhenli Liu, and Lingli Huang, and Yulian Wang, and Zonghui Yuan
Determination of multi-class pesticides in wines by solid-phase extraction and liquid chromatography-tandem mass spectrometry.
July 2009, Journal of chromatography. A,
Copied contents to your clipboard!