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3D printed metal columns for capillary liquid chromatography. 2014
S Sandron, and
B Heery, and
V Gupta, and
D A Collins, and
E P Nesterenko, and
P N Nesterenko, and
M Talebi, and
S Beirne, and
F Thompson, and
G G Wallace, and
D Brabazon, and
F Regan, and
B Paull
Australian Centre for Research on Separation Sciences (ACROSS), and ARC Centre of Excellence for Electromaterials Science, School of Physical Sciences, University of Tasmania, Australia. Brett.Paull@utas.edu.au.
Coiled planar capillary chromatography columns (0.9 mm I.D. × 60 cm L) were 3D printed in stainless steel (316L), and titanium (Ti-6Al-4V) alloys (external dimensions of ~5 × 30 × 58 mm), and either slurry packed with various sized reversed-phase octadecylsilica particles, or filled with an in situ prepared methacrylate based monolith. Coiled printed columns were coupled directly with 30 × 30 mm Peltier thermoelectric direct contact heater/cooler modules. Preliminary results show the potential of using such 3D printed columns in future portable chromatographic devices.
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