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Oxalyl amide assisted palladium-catalyzed arylation of C(sp2)-H bond at the δ position. 2014
Jian Han, and
Pei Liu, and
Chao Wang, and
Qian Wang, and
Jingyu Zhang, and
Yanwei Zhao, and
Daqing Shi, and
Zhibin Huang, and
Yingsheng Zhao
Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry, Chemical Engineering and Materials Science, Soochow University , Suzhou 215123, China.
A successful protocol has been developed for δ-arylation of β-arylethamines at the ortho position under mild conditions. The newly developed methodology first presents broad substrate scope, great functional group tolerance, and good to excellent yield in the synthesis of substituted β-arylethylamines. The transformation represents a practical advantage of oxalyl amide in assistance with C-H functionalization at a remote position.
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