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[2.2]Paracyclophane derivatives containing tetrathiafulvalene moieties. 2015

Laura G Sarbu, and Lucian G Bahrin, and Peter G Jones, and Lucian M Birsa, and Henning Hopf
Department of Chemistry, "Al. I. Cuza" University of Iasi, 11 Carol I Bv., RO-700506 Iasi, Romania ; Institute of Organic Chemistry, Technical University of Braunschweig, Hagenring 30, D-38106 Braunschweig, Germany.

The synthesis of [2.2]paracyclophane derivatives containing tetrathiafulvalene units has been accomplished by the coupling reaction of 4-([2.2]paracyclophan-4-yl)-1,3-dithiol-2-thione in the presence of trimethylphosphite. The 1,3-dithiol-2-thione derivative was in turn synthesized by the regioselective bromination of 4-acetyl[2.2]paracyclophane, then through the corresponding dithiocarbamates and 1,3-dithiolium salts.

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