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Crystal structure of aqua-tris-{μ-N-[bis(diethyl-amino)phosphoryl]-2,2,2-tri-chloroacetamidato-κ3O,O':O}calciumsodium. 2016
Iuliia Shatrava, and
Kateryna Gubina, and
Vladimir Ovchynnikov, and
Viktoriya Dyakonenko, and
Vladimir Amirkhanov
Taras Shevchenko National University of Kyiv, Department of Chemistry, Volodymyrska str., 64, 01033 Kyiv, Ukraine.
In the mol-ecular structure of the title compound, [CaNa(C10H20Cl3N3O2P)3(H2O)], the Ca2+ ion has a slightly distorted octa-hedral coordination environment defined by six O atoms which belong to the carbonyl and phosphoryl groups of the three coordinating ligands. Two Cl atoms of CCl3 groups and four O atoms form the coordination environment of the Na+ ion: three from the carbonyl groups of ligands and one O atom from a coordinating water mol-ecule. In the crystal, the bimetallic complexes are assembled into chains along the c-axis direction via O-H⋯O hydrogen bonds that involve the coordinating water mol-ecules and the phosphoryl groups.
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