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Copper- and Palladium-Catalyzed Cross-Coupling Reactions for the Synthesis of N-Fused Benzo[4,5]imidazo[2,1-b]thiazole Derivatives via Substituted trans-1,2-Diiodoalkenes, 1H-Benzo[d]imidazole-2-thiols, and Halobenzenes. 2017
Guodong Shen, and
Bingchuan Yang, and
Xianqiang Huang, and
Yaxin Hou, and
Huan Gao, and
Jichun Cui, and
Chuansheng Cui, and
Tongxin Zhang
School of Chemistry and Chemical Engineering, School of Pharmacy, Liaocheng University , Liaocheng, 252000 Shandong, P. R. China.
Two transition metal (Cu and Pd)-catalyzed C-S, C-N, and C-C bond cross-coupling reactions for the preparation of N-fused benzo[4,5]imidazo[2,1-b]thiazole derivatives were developed. A variety of 3-substituted and 2,3-disubstituted benzo[4,5]imidazo[2,1-b]thiazoles were efficiently and conveniently synthesized from the coupling reaction via trans-1,2-diiodoalkenes, 1H-benzo[d]imidazole-2-thiols, and halobenzenes in moderate to excellent yields.
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