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Asymmetric synthesis of CF3-containing tetrahydroquinoline via a thiourea-catalyzed cascade reaction. 2017
Yuanyuan Zhu, and
Boyu Li, and
Cui Wang, and
Zhenghao Dong, and
Xiaoling Zhong, and
Kairong Wang, and
Wenjin Yan, and
Rui Wang
The Institute of Pharmacology, Key Laboratory of Preclinical Study for New Drugs of Gansu Province, School of Basic Medical Sciences, Lanzhou University, Lanzhou 730000, China. yanwj@lzu.edu.cn wangrui@lzu.edu.cn.
An organocatalytic asymmetric method for the synthesis of 2-CF3 tetrahydroquinoline has been achieved. The cascade reaction of 2-aminochalcones with β-CF3 nitroalkenes afforded the products bearing three contiguous stereogenic centers in good yields with excellent diastereoselectivities and enantioselectivities.
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