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Well-defined BiOCl colloidal ultrathin nanosheets: synthesis, characterization, and application in photocatalytic aerobic oxidation of secondary amines. 2015

Yihui Wu, and Bo Yuan, and Mingrun Li, and Wen-Hua Zhang, and Yan Liu, and Can Li
State Key Laboratory of Catalysis , Dalian Institute of Chemical Physics , Chinese Academy of Sciences , Dalian National Laboratory for Clean Energy , Dalian 116023 , China . Email: whzhang@dicp.ac.cn ; Email: yanliu503@dicp.ac.cn ; Email: canli@dicp.ac.cn.

We demonstrate the first colloidal synthesis of single-crystalline BiOCl ultrathin nanosheets (UTNSs) that feature a well-defined square morphology. Unlike BiOCl nanomaterials prepared by hydrothermal routes, our colloidal BiOCl UTNSs exhibit hydrophobic surface properties and high activity and selectivity toward the photocatalytic aerobic oxidation of secondary amines to corresponding imines at room temperature. Hence, the application of BiOCl nanomaterials has been successfully extended from the widely studied photodecomposition of pollutants in aqueous solution to the synthesis of fine chemicals in organic solvent using a green approach.

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