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Asymmetric Total Synthesis of (-)-Maldoxin, a Common Biosynthetic Ancestor of the Chloropupukeananin Family. 2018
Takahiro Suzuki, and
Soichiro Watanabe, and
Muhammet Uyanik, and
Kazuaki Ishihara, and
Susumu Kobayashi, and
Keiji Tanino
Department of Chemistry, Faculty of Science , Hokkaido University , Sapporo , 060-0816 Hokkaido , Japan.
The total synthesis of pestheic acid based on an intramolecular SNAr reaction without a nitro group and the asymmetric synthesis of (-)-maldoxin by a catalytic enantioselective oxidative dearomatization of pestheic acid are described. The reactivity of (-)-maldoxin as a diene in the Diels-Alder reaction is also investigated.
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