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One-Pot Synthesis of 4-Sulfonyliminotetrahydropyrimidin-2-one Derivatives through a Copper-Catalyzed Tandem Reaction. 2018

Tao Tong, and Xin Wu, and Erfei Li, and Honglan Kang, and Xiaoxia Wang, and Xin Lv
Key Laboratory of the Ministry of Education for Advanced Catalysis Materials , Zhejiang Normal University , 688 Yingbin Road , Jinhua 321004 , China.

A novel and efficient synthesis of 4-iminotetrahydropyrimidin-2-one derivatives was developed through a Cu(I)-catalyzed three-component tandem reaction employing propargylamines, isocyanates, and sulfonyl azides as starting materials. A wide range of polysubstituted 4-sulfonyliminotetrahydropyrimidin-2-ones, which might be useful in biological chemistry and medicinal science, were conveniently and efficiently assembled in one pot.

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