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Polypeptide Nanoparticles Obtained from Emulsion Polymerization of Amino Acid N-Carboxyanhydrides. 2019
Jaco Jacobs, and
Dražen Pavlović, and
Hannah Prydderch, and
Mohammad-Amin Moradi, and
Emmanuel Ibarboure, and
Johan P A Heuts, and
Sebastien Lecommandoux, and
Andreas Heise
School of Chemical Sciences , Dublin City University , Glasnevin, Dublin 9 , Ireland.
Polypeptide nanoparticles were obtained by the miniemulsion polymerization of S-(o-nitrobenzyl)-l-cysteine (NBC) N-carboxyanhydride (NCA). Through process optimization, reaction conditions were identified that allowed the polymerization of the water sensitive NCA to yield nanoparticles of about 220 nm size. Subsequent UV-irradiation of the nanoparticle emulsions caused the in situ removal of the nitrobenzyl group and particle cross-linking through disulfide bond formation accompanied by the shrinkage of the particles.
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