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Alternating Copolymerization of Epoxides and Anhydrides Catalyzed by Aluminum Complexes. 2018
Marc Martínez de Sarasa Buchaca, and
Felipe de la Cruz-Martínez, and
Javier Martínez, and
Carlos Alonso-Moreno, and
Juan Fernández-Baeza, and
Juan Tejeda, and
Enrique Niza, and
José A Castro-Osma, and
Antonio Otero, and
Agustín Lara-Sánchez
Departamento de Química Inorgánica, Orgánica y Bioquímica-Centro de Innovación en Química Avanzada (ORFEO-CINQA), Facultad de Ciencias y Tecnologías Químicas, Universidad de Castilla-La Mancha, 13071 Ciudad Real, Spain.
The optimization of an organoaluminum catalytic system for the copolymerization of epoxides and anhydrides is presented. For this purpose, the influence of different variables in the process, such as catalysts, cocatalyst, solvent, or substrates, has been analyzed. Kinetic studies, a proposal for the catalytic mechanism, and full characterization of the copolymers obtained are also discussed. Finally, a new copolymer, poly(limonene succinate), obtained by the optimized catalytic system is reported.
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