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Docking of tetra-methyl zirconium to the surface of silica: a well-defined pre-catalyst for conversion of CO2 to cyclic carbonates. 2020
Walid Al Maksoud, and
Aya Saidi, and
Manoja K Samantaray, and
Edy Abou-Hamad, and
Albert Poater, and
Samy Ould-Chikh, and
Xianrong Guo, and
Erjia Guan, and
Tao Ma, and
Bruce C Gates, and
Jean-Marie Basset
King Abdullah University of Science & Technology, Physical Science and Engineering KAUST, 23955-6900, Thuwal, Saudi Arabia. jeanmarie.basset@kaust.edu.sa manoja.samantaray@kaust.edu.sa.
The metal complex (Zr(CH3)4(THF)2) has been fully synthesized, characterized and grafted onto partially dehydroxylated silica to give two surface species [([triple bond, length as m-dash]Si-O-)Zr(CH3)3(THF)2] (minor) and [([triple bond, length as m-dash]Si-O-)2Zr(CH3)2(THF)2] (major) which have been characterized by SS NMR, IR, and elemental analysis. These supported pre-catalysts exhibit the best conversion of CO2 to cyclic carbonates, as compared to the previously reported SOMC catalysts.
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