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Electrochemically shape-controlled synthesis of great stellated dodecahedral Au nanocrystals with high-index facets for nitrogen reduction to ammonia. 2020
Yu-Chen Jiang, and
Yu-Jie Mao, and
Jin Zou, and
Hong-Hui Wang, and
Feng Liu, and
Yong-Sheng Wei, and
Tian Sheng, and
Xin-Sheng Zhao, and
Lu Wei
School of Physics and Electronic Engineering, Jiangsu Normal University, Xuzhou 221116, China. lwei057@jsnu.edu.cn.
Au great stellated dodecahedra (GSD), one of the Kepler-Poinsot solids, are synthesized by an electrochemical double-step potential method in a choline chloride-urea based deep eutectic solvent. The as-synthesized Au GSD are bound by high-index {331} facets and exhibit excellent electrocatalytic performance for the nitrogen reduction reaction with a high NH3 yield rate (49.96 μg h-1 cm-2) and faradaic efficiency (28.59%) under ambient conditions.
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