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Thermospray liquid chromatographic-mass spectrometric method for the analysis of metribuzin and its metabolites. 1988
C E Parker, and
A V Geeson, and
D E Games, and
E D Ramsey, and
E O Abusteit, and
F T Corbin, and
K B Tomer
Laboratory of Molecular Biophysics, National Institute of Environmental Health Sciences, Research Triangle Park, NC 27709.
A thermospray liquid chromatographic-mass spectrometric (TSP LC-MS) method has been developed for the analysis of the herbicide metribuzin and its three major metabolites in plant tissue. Metribuzin and its metabolites exhibited widely varying sensitivities in positive-ion TSP, with metribuzin being the most sensitive and deaminated diketo metribuzin being the least sensitive. All four compounds of interest were detected in an extract of a soybean plant which had been treated with metribuzin.
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