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Postsynthetic Modification of Metal-Organic Frameworks by Vapor-Phase Grafting. 2021
Siyi Rong, and
Shizheng Chen, and
Pengcheng Su, and
Huiyu Tang, and
Miaomiao Jia, and
Yan Xia, and
Wanbin Li
Guangdong Key Laboratory of Environmental Pollution and Health, School of Environment, Jinan University, Guangzhou 511443, P. R. China.
A vapor-phase grafting strategy is developed for the postsynthetic modification of metal-organic frameworks (MOFs). On the basis of the Schotten-Baumann reaction between acyl chloride (-COCl) and amino (-NH2) groups and hydrolysis of -COCl, the carboxylated MOFs could be prepared through simple exposure in vaporized acyl chloride molecules and immersion in water. The modified MOFs have well-maintained crystalline structures and porosities and show substantially improved fluoride removal performance.
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