Dispersive Solid-Phase Extraction of Multiresidue Pesticides in Food and Water Samples. 2021

Hongxia Guan
School of Science and Technology, Georgia Gwinnett College, 1000 University Center Lane, Lawrenceville, GA, USA. sguan1@ggc.edu.

Pesticides has become an essential part of our life and have entered and bioaccumulated in water, air, soil ecosystem, and food. However, the majority of the pesticides are not biodegradable and eco-friendly, and the accumulation of them in food and the ecosystem could constitute a serious risk to human and environmental health. It is critical to understand pesticides' identities and level of residues present in environment and food. Robust analytical techniques that offer easy, fast, and reliable extraction of multiresidue pesticides in water, soil and food with matrix interference-free quantification are necessary for proper risk assessment. Although various methods have been reported for pesticides extraction in food and environment samples, dispersive solid-phase extraction (d-SPE) has become the most popular sample preparation method for pesticides analysis today. Multiresidue pesticides extraction in food and environmental sample using a novel d-SPE method, dispersive pipette extraction (DPX), is described step-by-step in this chapter.

UI MeSH Term Description Entries
D010575 Pesticides Chemicals used to destroy pests of any sort. The concept includes fungicides (FUNGICIDES, INDUSTRIAL); INSECTICIDES; RODENTICIDES; etc. Pesticide
D002523 Edible Grain SEEDS used as a major nutritional source, most often the grain from the POACEAE family. Cereals,Cereal Grain,Cereal,Cereal Grains,Edible Grains,Grain, Cereal,Grain, Edible,Grains, Cereal,Grains, Edible
D005502 Food Substances taken in by the body to provide nourishment. Foods
D005504 Food Analysis Measurement and evaluation of the components of substances to be taken as FOOD. Analysis, Food,Analyses, Food,Food Analyses
D005506 Food Contamination The presence in food of harmful, unpalatable, or otherwise objectionable foreign substances, e.g. chemicals, microorganisms or diluents, before, during, or after processing or storage. Food Adulteration,Adulteration, Food,Adulterations, Food,Contamination, Food,Contaminations, Food,Food Adulterations,Food Contaminations
D005638 Fruit The fleshy or dry ripened ovary of a plant, enclosing the seed or seeds. Berries,Legume Pod,Plant Aril,Plant Capsule,Aril, Plant,Arils, Plant,Berry,Capsule, Plant,Capsules, Plant,Fruits,Legume Pods,Plant Arils,Plant Capsules,Pod, Legume,Pods, Legume
D014675 Vegetables A food group comprised of EDIBLE PLANTS or their parts. Vegetable
D014867 Water A clear, odorless, tasteless liquid that is essential for most animal and plant life and is an excellent solvent for many substances. The chemical formula is hydrogen oxide (H2O). (McGraw-Hill Dictionary of Scientific and Technical Terms, 4th ed) Hydrogen Oxide
D014874 Water Pollutants, Chemical Chemical compounds which pollute the water of rivers, streams, lakes, the sea, reservoirs, or other bodies of water. Chemical Water Pollutants,Landfill Leachate,Leachate, Landfill,Pollutants, Chemical Water
D052616 Solid Phase Extraction An extraction method that separates analytes using a solid phase and a liquid phase. It is used for preparative sample cleanup before analysis by CHROMATOGRAPHY and other analytical methods. Extraction, Solid Phase,Extractions, Solid Phase,Solid Phase Extractions

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