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eFluorination Using Cheap and Readily Available Tetrafluoroborate Salts. 2023
Matthew C Leech, and
Dmitrii Nagornîi, and
Jamie M Walsh, and
Cyrille Kiaku, and
Darren L Poole, and
Joseph Mason, and
Iain C A Goodall, and
Perry Devo, and
Kevin Lam
School of Science, Faculty of Engineering and Science, University of Greenwich, Chatham Maritime, Kent ME4 4TB, United Kingdom.
A practical electrochemical method for the rapid, safer, and mild synthesis of tertiary hindered alkyl fluorides from carboxylic acids has been developed without the need for hydrofluoric acid salts or non-glass reactors. In this anodic fluorination, collidinium tetrafluoroborate acts as both the supporting electrolyte and fluoride donor. A wide range of functional groups has been shown to be compatible, and the possibility of scale-up using flow electrochemistry has also been demonstrated.
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