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Preparation of [68Ga]Ga-Chloride from 68Zn solid target for the synthesis of pharmaceutical grade [68Ga]Ga-PSMA-11 and [68Ga]Ga-DOTA-TATE. 2023
Sankha Chattopadhyay, and
Shayantani Ash, and
D G Mahesh, and
Luna Barua, and
Arpit Mitra, and
Sujata Saha Das, and
Samarjit Singha, and
Md Alam Nayer, and
Madhusmita, and
Umesh Kumar, and
Samarendu Sinha
Medical Cyclotron Facility, Regional Centre, Board of Radiation and Isotope Technology, VECC, Kolkata, India. Electronic address: sankha@vecc.gov.in.
68Ga is produced from enriched zinc-68 target electrodeposited on copper base material which was irradiated with 15 MeV proton energy in 30 MeV cyclotron. A modified semi-automated separation and purification module was used to obtain pharmaceutical grade [68Ga]GaCl3 in 35 ± 5 min. The quality of [68Ga]GaCl3 produced was in accordance with Pharmeuropa 30.4. The [68Ga]GaCl3 was utilized for the formulation of multiple doses of [68Ga]Ga-PSMA-11 and [68Ga]Ga-DOTATATE. The quality of [68Ga]Ga-PSMA-11 and [68Ga]Ga-DOTATATE were also in accordance with Pharmacopeia.
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