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Three-Component Reaction between 3-Acetylcoumarins, Amines, and Elemental Sulfur: A Designed Approach to 3-Amino-4H-thieno[3,2-c]coumarins. 2024
Behnaz Farajpour, and
Roujin Heydarzadeh, and
Faiq H S Hussain, and
Behrouz Notash, and
Peiman Mirzaei, and
Morteza Shiri
Department of Organic Chemistry, Faculty of Chemistry, Alzahra University, Vanak, Tehran 1993893973, Iran.
In this work, a series of novel 3-amino-4H-thieno[3,2-c]coumarins were designed and synthesized by a one-pot, catalyst-free, and three-component reaction of 3-acetylcoumarins with amines and elemental sulfur. Readily available starting materials, simple heating conditions, facile installation of a sulfur atom into the molecule using S8 as a sulfur source, acceptable functional group tolerance, and synthetically useful yields are some highlighted benefits of this process.
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