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Visible-Light-Promoted Deoxygenative Alkylation of Quinoxalin-2(1H)-ones with Activated Alcohols. 2024
Lili Wang, and
Pengyuan Yang, and
Jinwei Yuan, and
Wei Lian, and
Xinrong Jin, and
Sanyu Zhang, and
Liangru Yang, and
Dongliang Xing
School of Chemistry and Chemical Engineering, Henan University of Technology, Zhengzhou 450001, P. R. China.
A one-pot strategy for deoxygenative alkylation of alcohols with quinoxalin-2(1H)-ones was developed by using xanthate salts as alcohol-activating groups for radical generation in the presence of tricyclohexylphosphine under visible-light-promoted conditions. The remarkable features of this reaction include a broad substrate scope, excellent functional group tolerance, mild conditions, and simple operation. Moreover, the synthetic utility of this reaction was validated by the success of two-step one-pot reactions, scale-up synthesis, and chemoselective radical monodeoxygenation of diols.
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