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Synthesis and crystal structure of 2,9-di-amino-5,6,11,12-tetra-hydro-dibenzo[a,e]cyclo-octene. 2024

Nichole Valdez, and Eric Nagel, and Erica Redline, and Mark Rodriguez, and Chad Staiger, and Jason Dugger, and Jeffrey Foster
Sandia National Laboratories, 1515 Eubank Blvd. SE, Albuquerque, NM 87123, USA.

The cis- form of di-amino-dibenzo-cyclo-octane (DADBCO, C16H18N2) is of inter-est as a negative coefficient of thermal expansion (CTE) material. The crystal structure was determined through single-crystal X-ray diffraction at 100 K and is presented herein.

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