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A gas chromatographic method is described for the determination of deoxynivalenol (DON) and its metabolite DOM-1 in milk. Milk samples were extracted with ethyl acetate on a commercially available disposable extraction column, followed by hexane-acetonitrile partitioning. Final purification was accomplished on a reverse phase C-18 cartridge. The trimethylsilyl ether (TMS) derivatives of DON were prepared, chromatographed on an OV-17 column, and quantitated with an electron capture detector. Chromatography of the TMS derivatives of milk extracts was compared to that of the corresponding heptafluorobutyryl derivatives. The limit of detection using TMS derivatives was 1 ng/mL for both toxins with recoveries averaging 82% +/- 9% at 2.5 and 10 ng/mL milk for DON and 85% +/- 6% at 10 ng/mL for DOM-1.
S P Swanson, and
A M Dahlem, and
H D Rood, and
L M Côte, and
W B Buck, and
T Yoshizawa
April 1987,
Food and chemical toxicology : an international journal published for the British Industrial Biological Research Association,
S P Swanson, and
A M Dahlem, and
H D Rood, and
L M Côte, and
W B Buck, and
T Yoshizawa
January 1972,
Journal of agricultural and food chemistry,
S P Swanson, and
A M Dahlem, and
H D Rood, and
L M Côte, and
W B Buck, and
T Yoshizawa
July 1988,
Journal of chromatography,
S P Swanson, and
A M Dahlem, and
H D Rood, and
L M Côte, and
W B Buck, and
T Yoshizawa
January 1990,
Journal de toxicologie clinique et experimentale,
S P Swanson, and
A M Dahlem, and
H D Rood, and
L M Côte, and
W B Buck, and
T Yoshizawa
December 1986,
Zeitschrift fur Lebensmittel-Untersuchung und -Forschung,
S P Swanson, and
A M Dahlem, and
H D Rood, and
L M Côte, and
W B Buck, and
T Yoshizawa
November 1983,
Journal - Association of Official Analytical Chemists,
S P Swanson, and
A M Dahlem, and
H D Rood, and
L M Côte, and
W B Buck, and
T Yoshizawa
February 2017,
Mycotoxin research,
S P Swanson, and
A M Dahlem, and
H D Rood, and
L M Côte, and
W B Buck, and
T Yoshizawa
August 2021,
Journal of applied toxicology : JAT,
S P Swanson, and
A M Dahlem, and
H D Rood, and
L M Côte, and
W B Buck, and
T Yoshizawa
September 1973,
Nihon yakurigaku zasshi. Folia pharmacologica Japonica,
S P Swanson, and
A M Dahlem, and
H D Rood, and
L M Côte, and
W B Buck, and
T Yoshizawa
October 1978,
Clinical chemistry,
