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The low resolution mass spectra of E-3,4-bis-(p-hydroxyphenyl)-hex-3-ene (diethylstilbestrol), E-[1,1,1-3H3]3,4-bis-(p-hydroxyphenyl)-hex-3-ene, E-2,3-bis-(p-hydroxyphenyl)-but-2-ene (dimethylstilbestrol), E,E-3,4-bis-(p-hydroxyphenyl)hexa-2,4-diene (dienestrol) and 3,4-bis-(p-hydroxyphenyl)-hexane (hexestrol) were examined as the parent compounds, their diacetates, dimethyl ethers, and bis-trimethylsilyl ethers. In addition, the mass spectra of the diethyl ether and the hexadeuteriodimethyl ether of E-3,4-bis-(p-hydroxyphenyl)-hex-3-ene were studied. Each compound gives rise to several sets of characteristic fragment ions associated with loss of alkyl groups, loss of aryl groups and rearrangements. An ion of m/e 165 (C13H9) was found in the spectra of all the compounds studied. With the aid of high resolution mass spectrometry empirical formulae were assigned to major ions of the free diphenols.
L L Engel, and
P J Marshall, and
J C Orr, and
V N Reinhold, and
P Carter
June 1970,
Analytical biochemistry,
L L Engel, and
P J Marshall, and
J C Orr, and
V N Reinhold, and
P Carter
April 1975,
Bollettino chimico farmaceutico,
L L Engel, and
P J Marshall, and
J C Orr, and
V N Reinhold, and
P Carter
January 1971,
Journal of the Chemical Society. Perkin transactions 1,
L L Engel, and
P J Marshall, and
J C Orr, and
V N Reinhold, and
P Carter
September 1977,
Carbohydrate research,
L L Engel, and
P J Marshall, and
J C Orr, and
V N Reinhold, and
P Carter
May 1967,
Journal of the American Chemical Society,
L L Engel, and
P J Marshall, and
J C Orr, and
V N Reinhold, and
P Carter
May 1969,
Proceedings of the National Academy of Sciences of the United States of America,
L L Engel, and
P J Marshall, and
J C Orr, and
V N Reinhold, and
P Carter
January 1959,
Journal of research of the National Bureau of Standards. Section A, Physics and chemistry,
L L Engel, and
P J Marshall, and
J C Orr, and
V N Reinhold, and
P Carter
January 1975,
Journal of the Chemical Society. Perkin transactions 1,
L L Engel, and
P J Marshall, and
J C Orr, and
V N Reinhold, and
P Carter
October 1950,
Chemical reviews,
L L Engel, and
P J Marshall, and
J C Orr, and
V N Reinhold, and
P Carter
November 1971,
International journal of environmental analytical chemistry,
