A new method for determination of oxalate in blood serum by gas chromatography. 1978

P Nuret, and M Offner

A method for the determination of blood oxalate by gas chromatography is described. After clarification of the serum with acetone, the oxalate was extracted, ethylated and analysed on a gas chromatograph. The concentration of oxalate in the sample was determined by comparison with the elution pattern of diethylmalonate used as an internal standard. Using this technique, the recovery of added oxalate was more than 80%. Normal subjects were found to have blood oxalate levels of 27 mumol/l or less.

UI MeSH Term Description Entries
D008832 Microchemistry The development and use of techniques and equipment to study or perform chemical reactions, with small quantities of materials, frequently less than a milligram or a milliliter.
D010070 Oxalates Derivatives of OXALIC ACID. Included under this heading are a broad variety of acid forms, salts, esters, and amides that are derived from the ethanedioic acid structure. Oxalate,Ethanedioic Acids,Oxalic Acids,Acids, Ethanedioic,Acids, Oxalic
D002849 Chromatography, Gas Fractionation of a vaporized sample as a consequence of partition between a mobile gaseous phase and a stationary phase held in a column. Two types are gas-solid chromatography, where the fixed phase is a solid, and gas-liquid, in which the stationary phase is a nonvolatile liquid supported on an inert solid matrix. Chromatography, Gas-Liquid,Gas Chromatography,Chromatographies, Gas,Chromatographies, Gas-Liquid,Chromatography, Gas Liquid,Gas Chromatographies,Gas-Liquid Chromatographies,Gas-Liquid Chromatography
D006801 Humans Members of the species Homo sapiens. Homo sapiens,Man (Taxonomy),Human,Man, Modern,Modern Man

Related Publications

P Nuret, and M Offner
January 1977, Clinical chemistry,
P Nuret, and M Offner
November 1978, Journal of chromatography,
P Nuret, and M Offner
October 1987, Journal of chromatography,
P Nuret, and M Offner
June 1983, The Journal of urology,
P Nuret, and M Offner
April 1985, Nihon Hinyokika Gakkai zasshi. The japanese journal of urology,
P Nuret, and M Offner
January 1981, Laboratornoe delo,
P Nuret, and M Offner
January 1995, Annales de biologie clinique,
P Nuret, and M Offner
November 1975, American Industrial Hygiene Association journal,
P Nuret, and M Offner
November 1971, Nihon Sanka Fujinka Gakkai zasshi,
Copied contents to your clipboard!