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Equilibration of the phosphorus in radioactive phosphoric acid with the phosphorus in phosphorus oxychloride occurs if these compounds are refluxed together for approximately 24 h. This observation led us to develop a method for the preparation of radioactive phosphorus oxychloride on a small scale with high specific radioactivity. The labeled phosphorus oxychloride may be utilized directly in a one-pot reaction for the preparation of labeled phosphate esters or for the synthesis of more selective phosphorylating agents such as cyanoethyl phosphate. Since the method is very simple and capable of yielding highly labeled radioactive phosphate esters on a small scale, it is applicable to a number of different problems. The preparation of 32P-labeled dolichyl phosphate is described utilizing this procedure.
R W Keenan, and
R A Martinez, and
R F Williams
October 1976,
Chemistry and physics of lipids,
R W Keenan, and
R A Martinez, and
R F Williams
May 1986,
Analytical biochemistry,
R W Keenan, and
R A Martinez, and
R F Williams
August 2007,
European journal of nuclear medicine and molecular imaging,
R W Keenan, and
R A Martinez, and
R F Williams
January 1978,
Methods in enzymology,
R W Keenan, and
R A Martinez, and
R F Williams
January 1955,
Archiv der Pharmazie und Berichte der Deutschen Pharmazeutischen Gesellschaft,
R W Keenan, and
R A Martinez, and
R F Williams
June 1979,
Analytical biochemistry,
R W Keenan, and
R A Martinez, and
R F Williams
February 1993,
Analytical biochemistry,
R W Keenan, and
R A Martinez, and
R F Williams
October 1982,
The Biochemical journal,
R W Keenan, and
R A Martinez, and
R F Williams
March 1967,
Yakugaku zasshi : Journal of the Pharmaceutical Society of Japan,
R W Keenan, and
R A Martinez, and
R F Williams
December 1983,
The Journal of biological chemistry,
