Microwave digestion-inductively coupled plasma atomic emission spectrometric determination of boron in raw noodles. 1995

J Ziaziaris, and J L Kacprzak
New South Wales Health Department, Division of Analytical Laboratories, Lidcombe, Australia.

Samples of raw noodles in a mixture of nitric acid and hydrogen peroxide were microwave digested in sealed tetrafluoromethaxil (PTFE TFM) vessels. The digests were diluted to volume with distilled water and quantitated by inductively coupled plasma atomic emission spectroscopy (ICP-AES). The recoveries of boron for spikes of 2.5, 250, and 500 micrograms were 88, 101, and 102%, respectively. The quantitation limit was estimated to be 1.5 mg B/kg. The method is rapid and ideally suited to large numbers of samples.

UI MeSH Term Description Entries
D008872 Microwaves That portion of the electromagnetic spectrum from the UHF (ultrahigh frequency) radio waves and extending into the INFRARED RAYS frequencies. EHF Waves,Extremely High Frequency Radio Waves,Micro Wave,Micro Waves,Ultrahigh Frequency Waves,Microwave Radiation,EHF Wave,Micro Waves,Microwave,Microwave Radiations,Radiation, Microwave,Ultrahigh Frequency Wave,Wave, EHF,Wave, Micro,Wave, Ultrahigh Frequency,Waves, Micro
D001895 Boron A trace element with the atomic symbol B, atomic number 5, and atomic weight [10.806; 10.821]. Boron-10, an isotope of boron, is used as a neutron absorber in BORON NEUTRON CAPTURE THERAPY. Boron-11,Boron 11
D005504 Food Analysis Measurement and evaluation of the components of substances to be taken as FOOD. Analysis, Food,Analyses, Food,Food Analyses
D012680 Sensitivity and Specificity Binary classification measures to assess test results. Sensitivity or recall rate is the proportion of true positives. Specificity is the probability of correctly determining the absence of a condition. (From Last, Dictionary of Epidemiology, 2d ed) Specificity,Sensitivity,Specificity and Sensitivity
D013053 Spectrophotometry The art or process of comparing photometrically the relative intensities of the light in different parts of the spectrum.

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