[Methods for determining boron compounds in the air of a work area]. 1994

V Gŭlŭbova

The studies performed with the chinalizarin method the for determination of the concentration of boric compounds in the air of the working area, proved to be impracticable in the presence of geranium and beryllium compounds. A spectrometric method for analysis of boric compounds was developed, based on their interaction with fluoric and ferric ions in the presence of sulfo-salicylic acid, and a complex compound was received of light orange colour to red, depending on the boric concentration. The maximum of absorption was at wave length of 577 mm. The sensitivity of the method was 0.001 mg boric in the analyzed sample -2 cm3. There is a linear dependence between the boric concentration and the optic density of the developed samples of interval 0.001-0.15 mg borium. The accuracy of the method expressed by coefficient of variation in % is in interval 12.4-6.3% for borium concentrations of 0.001-0.1 mg. The field where the method could be applied is defined in the presence of titanium, copper and lead compounds.

UI MeSH Term Description Entries
D007202 Indicators and Reagents Substances used for the detection, identification, analysis, etc. of chemical, biological, or pathologic processes or conditions. Indicators are substances that change in physical appearance, e.g., color, at or approaching the endpoint of a chemical titration, e.g., on the passage between acidity and alkalinity. Reagents are substances used for the detection or determination of another substance by chemical or microscopical means, especially analysis. Types of reagents are precipitants, solvents, oxidizers, reducers, fluxes, and colorimetric reagents. (From Grant & Hackh's Chemical Dictionary, 5th ed, p301, p499) Indicator,Reagent,Reagents,Indicators,Reagents and Indicators
D001896 Boron Compounds Inorganic or organic compounds that contain boron as an integral part of the molecule. Borides,Compounds, Boron
D003124 Colorimetry Any technique by which an unknown color is evaluated in terms of standard colors. The technique may be visual, photoelectric, or indirect by means of spectrophotometry. It is used in chemistry and physics. (McGraw-Hill Dictionary of Scientific and Technical Terms, 4th ed)
D004347 Drug Interactions The action of a drug that may affect the activity, metabolism, or toxicity of another drug. Drug Interaction,Interaction, Drug,Interactions, Drug
D005857 Germanium A rare metal element with a blue-gray appearance and atomic symbol Ge, atomic number 32, and atomic weight 72.63.
D000395 Air Pollutants, Occupational Toxic air-borne matter related to work performed They are usually produced by the specific nature of the occupation. Occupational Air Pollutants,Pollutants, Occupational Air
D012680 Sensitivity and Specificity Binary classification measures to assess test results. Sensitivity or recall rate is the proportion of true positives. Specificity is the probability of correctly determining the absence of a condition. (From Last, Dictionary of Epidemiology, 2d ed) Specificity,Sensitivity,Specificity and Sensitivity
D013053 Spectrophotometry The art or process of comparing photometrically the relative intensities of the light in different parts of the spectrum.

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