Gas-liquid chromatographic determination of beta-asarone in wine: collaborative study. 1977

R H Dyer

The gas-liquid chromatographic determination of beta-asarone (cis-2,4,5-trimethyoxy-1-propenylbenzene) in wine was collaboratively studied by 9 analysts. The samples were first distilled and then extracted into hexane prior to chromatography. The mean recovery for 8 spiked samples, analyzed as blind duplicates, was 89.27%. The reproducibility coefficient of variation was 17.9%, and the repeatability coefficient of variation was 8.3%. No unfavorable remarks were noted. The method has been adopted as official first action.

UI MeSH Term Description Entries
D002849 Chromatography, Gas Fractionation of a vaporized sample as a consequence of partition between a mobile gaseous phase and a stationary phase held in a column. Two types are gas-solid chromatography, where the fixed phase is a solid, and gas-liquid, in which the stationary phase is a nonvolatile liquid supported on an inert solid matrix. Chromatography, Gas-Liquid,Gas Chromatography,Chromatographies, Gas,Chromatographies, Gas-Liquid,Chromatography, Gas Liquid,Gas Chromatographies,Gas-Liquid Chromatographies,Gas-Liquid Chromatography
D005421 Flavoring Agents Substances added to foods and medicine to improve the taste. Flavor Additives,Flavor Enhancers,Additive, Flavor,Additives, Flavor,Agent, Flavoring,Agents, Flavoring,Enhancer, Flavor,Enhancers, Flavor,Flavor Additive,Flavor Enhancer,Flavoring Agent
D000840 Anisoles A group of compounds that are derivatives of methoxybenzene and contain the general formula R-C7H7O. Methylphenyl Ethers,Ethers, Methylphenyl
D014920 Wine Fermented juice of fresh grapes or of other fruit or plant products used as a beverage. Wines

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