Technique for generating submicrometer ultra high molecular weight polyethylene particles. 1996

A S Shanbhag, and C T Hasselman, and H E Rubash
Department of Orthopaedic Surgery, University of Pittsburgh, Pennsylvania, USA. arshan+@pitt.edu

Ultra high molecular weight polyethylene wear debris is believed to have a major role in aseptic loosening of prosthetic joints. In order to study the cellular and host response to this and other such particulate debris, a source of fine ultra high molecular weight polyethylene debris is needed. We have described a technique to fracture the GUR 4150 primary ultra high molecular weight polyethylene grain, which reproducibly generated particles less than 1 micron in size. Furthermore, the particle morphology was similar to that of ultra high molecular weight polyethylene particles generated in vivo and retrieved from interfacial tissues. The fabricated polyethylene particles ranged from 0.1 to 33 microns in diameter, with a mean of 2.3 +/- 0.2 micron. Sixty percent of the particles were smaller than 1 micron and 90% were smaller than 7 microns. Using filtration and sedimentation, it is possible to acquire finer particle fractions. These particles are currently being used for biological response studies.

UI MeSH Term Description Entries
D008855 Microscopy, Electron, Scanning Microscopy in which the object is examined directly by an electron beam scanning the specimen point-by-point. The image is constructed by detecting the products of specimen interactions that are projected above the plane of the sample, such as backscattered electrons. Although SCANNING TRANSMISSION ELECTRON MICROSCOPY also scans the specimen point by point with the electron beam, the image is constructed by detecting the electrons, or their interaction products that are transmitted through the sample plane, so that is a form of TRANSMISSION ELECTRON MICROSCOPY. Scanning Electron Microscopy,Electron Scanning Microscopy,Electron Microscopies, Scanning,Electron Microscopy, Scanning,Electron Scanning Microscopies,Microscopies, Electron Scanning,Microscopies, Scanning Electron,Microscopy, Electron Scanning,Microscopy, Scanning Electron,Scanning Electron Microscopies,Scanning Microscopies, Electron,Scanning Microscopy, Electron
D008970 Molecular Weight The sum of the weight of all the atoms in a molecule. Molecular Weights,Weight, Molecular,Weights, Molecular
D009985 Orthopedics A specialty which utilizes medical, surgical, and physical methods to treat and correct deformities, diseases, and injuries to the skeletal system, its articulations, and associated structures.
D010316 Particle Size Relating to the size of solids. Particle Sizes,Size, Particle,Sizes, Particle
D011095 Polyethylenes Synthetic thermoplastics that are tough, flexible, inert, and resistant to chemicals and electrical current. They are often used as biocompatible materials for prostheses and implants. Ethylene Polymers,Ethene Homopolymers,Homopolymers, Ethene,Polymers, Ethylene

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