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A fast and reliable method for the determination of polychlorinated biphenyls (PCBs) and chlorinated pesticides in human body fluids and tissues is presented. Sample clean-up and selective enrichment of analytes are carried out by liquid column chromatography without a prior solvent extraction step. Analytes are determined either by high-resolution capillary gas chromatography with mass spectrometric detection, or by dual-column GC followed by electron-capture detection. A procedure is described for the simultaneous determination of environmental levels of the PCB congeners 28, 52, 101, 138, 153 and 180 in human cord serum. The method allows the simultaneous determination of chlorinated pesticides such as aldrin, DDT, DDE, BHC and HCB and is also applicable to other biological matrices, such as bone marrow or tissues.
K A Bucholski, and
J Begerow, and
G Winneke, and
L Dunemann
October 2012,
Chemosphere,
K A Bucholski, and
J Begerow, and
G Winneke, and
L Dunemann
May 1996,
Central European journal of public health,
K A Bucholski, and
J Begerow, and
G Winneke, and
L Dunemann
January 1990,
Journal of analytical toxicology,
K A Bucholski, and
J Begerow, and
G Winneke, and
L Dunemann
January 1978,
Arhiv za higijenu rada i toksikologiju,
K A Bucholski, and
J Begerow, and
G Winneke, and
L Dunemann
April 1967,
Industrial medicine & surgery,
K A Bucholski, and
J Begerow, and
G Winneke, and
L Dunemann
May 1999,
Ecotoxicology and environmental safety,
K A Bucholski, and
J Begerow, and
G Winneke, and
L Dunemann
January 1971,
Journal - Association of Official Analytical Chemists,
K A Bucholski, and
J Begerow, and
G Winneke, and
L Dunemann
July 1980,
Journal - Association of Official Analytical Chemists,
K A Bucholski, and
J Begerow, and
G Winneke, and
L Dunemann
January 1988,
Journal - Association of Official Analytical Chemists,
K A Bucholski, and
J Begerow, and
G Winneke, and
L Dunemann
January 1970,
Acta chemica Scandinavica,
