Storage stability of dental luting agents. 1999

S O Hondrum
US Army Dental Laboratory, Fort Gordon, Ga 30905-5661, USA. SHondrum@aol.com

BACKGROUND Mechanical properties are considered to be important to the clinical success of dental cements. Storage time of dental luting agents (dental cements) before use and at the manufacturer may have substantial effects on their properties. OBJECTIVE This study observed and investigated the changes in the properties of water-based dental luting agents over time and on exposure to various environmental conditions. METHODS Properties of zinc phosphate, zinc polycarboxylate, and glass-ionomer luting agents were recorded at baseline and at intervals past 84 months, whereas the materials were exposed to controlled storage conditions as well as various conditions typical of clinical situations. Tests included viscosity, diametral tensile strength, ultimate compressive strength, rigidity, hardness, and working/setting times. RESULTS Viscosity increased over 24 to 60 months for the acidic polymer liquids (zinc polycarboxylate and glass ionomer). Tensile and compressive strengths began to decrease after 36 months for all cements, most acutely for glass ionomer. CONCLUSIONS Changes in critical properties on aging may not be noticed by the clinician and yet may impact clinical success. These data emphasize the importance of storage stability for perishable dental materials and portend the need for standardized tests.

UI MeSH Term Description Entries
D008422 Materials Testing The testing of materials and devices, especially those used for PROSTHESES AND IMPLANTS; SUTURES; TISSUE ADHESIVES; etc., for hardness, strength, durability, safety, efficacy, and biocompatibility. Biocompatibility Testing,Biocompatible Materials Testing,Hemocompatibility Testing,Testing, Biocompatible Materials,Testing, Hemocompatible Materials,Hemocompatibility Testings,Hemocompatible Materials Testing,Materials Testing, Biocompatible,Materials Testing, Hemocompatible,Testing, Biocompatibility,Testing, Hemocompatibility,Testing, Materials,Testings, Biocompatibility
D002850 Chromatography, Gel Chromatography on non-ionic gels without regard to the mechanism of solute discrimination. Chromatography, Exclusion,Chromatography, Gel Permeation,Chromatography, Molecular Sieve,Gel Filtration,Gel Filtration Chromatography,Chromatography, Size Exclusion,Exclusion Chromatography,Gel Chromatography,Gel Permeation Chromatography,Molecular Sieve Chromatography,Chromatography, Gel Filtration,Exclusion Chromatography, Size,Filtration Chromatography, Gel,Filtration, Gel,Sieve Chromatography, Molecular,Size Exclusion Chromatography
D003738 Dental Cements Substances used to bond COMPOSITE RESINS to DENTAL ENAMEL and DENTIN. These bonding or luting agents are used in restorative dentistry, ROOT CANAL THERAPY; PROSTHODONTICS; and ORTHODONTICS. Dental Adhesives,Luting Agents,Orthodontic Adhesives,Cement, Dental,Cements, Dental,Dental Cement,Adhesive, Dental,Adhesive, Orthodontic,Adhesives, Dental,Adhesives, Orthodontic,Dental Adhesive,Luting Agent,Orthodontic Adhesive
D004355 Drug Stability The chemical and physical integrity of a pharmaceutical product. Drug Shelf Life,Drugs Shelf Lives,Shelf Life, Drugs,Drug Stabilities,Drugs Shelf Life,Drugs Shelf Live,Life, Drugs Shelf,Shelf Life, Drug,Shelf Live, Drugs,Shelf Lives, Drugs
D004356 Drug Storage The process of keeping pharmaceutical products in an appropriate location. Drug Storages,Storage, Drug,Storages, Drug
D000704 Analysis of Variance A statistical technique that isolates and assesses the contributions of categorical independent variables to variation in the mean of a continuous dependent variable. ANOVA,Analysis, Variance,Variance Analysis,Analyses, Variance,Variance Analyses
D013997 Time Factors Elements of limited time intervals, contributing to particular results or situations. Time Series,Factor, Time,Time Factor

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